Experimental Station 9-2

Beam line 9-2 is a wiggler end station dedicated for monochromatic, high-throughput and high-resolution macromolecular crystallography and optimized for SAD and MAD experiments. It can be run in a full remote access mode.  It is equipped with a Dectris Pilatus 6M PAD detector and a remote access controlled UV-Vis  microspectrophotometer. For aditional information about the experimental capabilities, see http://smb.slac.stanford.edu/index.shtml.

Status
Open
Supported Techniques
Macromolecular Crystallography
Multi wavelength anomalous diffraction (MAD)
Single wavelength anomalous diffraction (SAD)
Main Scientific Disciplines
Biomedical Sciences
Bioscience
Structural Molecular Biology
Beam Line Specifications

Source

16-pole Wiggler

  Energy Range Resolution ΔE/E Spot Size Flux
Focused 6.0 - 14.0 keV ~3 x 10-4 H: 0.050-0.150 mm
W: 0.080-0.200 mm
5 x 1011

See also: BioSync 9-2

Optics

Mirror: Rh coated flat bent M0, toroidal focusing post-monochromator M1

Monochromator: Si(111) and Si(220) double crystal
 

Absorption

N/A

Instrumentation

Detector:  Dectris Pilatus 6M, pixel, sample to detector distance of 198-650 mm, shutterless data collection, fine phi slicing experiments

Goniometer: SSRL single-axis microdiffractometer, air bearing, coaxial cold stream, 1.5 micron SOC

Cryo Capability:  Oxford Cryojet

Microspectrophotometer: UV-VIS

Sample Environment

Ambient pressure. 

Sample temperature: 100K - room temperature.

Data Acquisition and Analysis

The beam line control GUI Blu-ice is installed at all the macromolecular crystallography beam lines. Web-ice provides an interface for diffraction image viewing and automated autoindex and data collection strategy calculation.

Other supported software installed on servers accessible from all the beamlines include mosflm, HKL2000 and XDS. MAD/SAD scripts, developed at SSRL, are also available to facilitate on-line structure solution. The graphics package COOT is installed on the local beamline computers.

 

Beam Line Phone
650-926-5292. Support cell phone: 650-714-9417
Beam Line Contact

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